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Ball milling under atmosphere

Jun 17, 2021 Apr 29, 2019 The solution-based reaction in dry THF and under nitrogen atmosphere at 50 C with either zinc flakes or granular zinc no additive used resulted in low yields of 7 and 4 , respectively Scheme 4 B, whereas under ball-milling conditions without any solvent, inert gas, or additive Table 2, the reaction proceeded smoothly in 2 h and all

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